PokéBase - Pokémon Q&A
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According to Serebii, you can't get it Emerald, Ruby, or Sapphire. Dang.

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You cannot find Dragon Scale as an item in Pokemon Emerald
However, you do have a 5% chance of finding them on Horsea, Seadra, Dratini, Dragonair, Dragonite, Kingdra, Shelgon, Bagon and Salamence after catching them.

http://www.serebii.net/itemdex/dragonscale.shtml

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